Interaction of d-treo-2-methylamino-1-phenyl-1-propanol with 4-morpholylbenzaldehyde in the conditions of convectional heating and microwave activation

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dc.contributor.author Fazylov, S.D.
dc.contributor.author Nurkenov, О.А.
dc.contributor.author Kulakov, I.V.
dc.contributor.author Arinova, А.E.
dc.contributor.author Satpayeva, Zh.B.
dc.contributor.author Zakarin, S.Z.
dc.contributor.author Issayeva, A.Zh.
dc.contributor.author Karipova, G.Zh.
dc.contributor.author Issabekova, D.S.
dc.date.accessioned 2019-03-07T06:00:48Z
dc.date.available 2019-03-07T06:00:48Z
dc.date.issued 2015-09-30
dc.identifier.citation Interaction of d-treo-2-methylamino-1-phenyl-1-propanol with 4-morpholylbenzaldehyde in the conditions of convectional heating and microwave activation/ S.D.Fazylov [et al.]// Қарағанды универисетінің хабаршысы. ХИМИЯ Сериясы.=Вестник Карагандинского университета. Серия ХИМИЯ.=Bulletin of the Karaganda University. CHEMISTRY Series. – 2015. – № 3.– C.9 -13. ru_RU
dc.identifier.issn 0142-0843
dc.identifier.uri http://rep.ksu.kz:80//handle/data/4105
dc.description.abstract The synthesis of 1,3-oxazolidine was made by condensation reaction of d-treo-2-methylamino-1-phenyl-1- propanol with 4-(N-morpholyl)-benzaldehyde under the conditions of convectional and microwave activation. The structure of 1,3-oxazolidine has been proved by IR- and 1Н NMR-spectroscopies. Physico-chemical constants of the oxazolidine obtained by both methods were identical. 4-(N-morpholyl)-benzaldehyde, 4-(4- ((4R,5R)-3,4-dimethyl-5-phenyloxazolidine-2-yl)phenyl)morpholine obtained very promising in terms of learning conformational features of the structure and biological properties. The structure of the new heterocyclic compounds — 4-(N-morpholyl)-benzaldehyde, 4-(4-((4R,5R)-3,4-dimethyl-5-phenyloxazolidine-2-yl)- phenyl)morpholine is proved by data IR and NMR 1H spectroscopy, as well as a comparative study of the influence of convection and microwave heating on the yield and character formation of the final product has been made. ru_RU
dc.language.iso en ru_RU
dc.publisher KSU Publ. ru_RU
dc.relation.ispartofseries Қарағанды универисетінің хабаршысы. ХИМИЯ Сериясы.=Вестник Карагандинского университета. Серия ХИМИЯ.=Bulletin of the Karaganda University. CHEMISTRY Series.;№ 3(79)/2015
dc.subject 1,3-oxazolidines ru_RU
dc.subject alkaloid of d-pseudoethedrine ru_RU
dc.subject β-aminoalcohols ru_RU
dc.subject 4-morpholinephenylic ru_RU
dc.subject tetramethylsilane ru_RU
dc.subject 4-(4-((4R,5R)-3,4-dimethyl-5-phenyloxazolidine- 2-yl)phenyl)morpholine ru_RU
dc.subject spin-spin interaction ru_RU
dc.title Interaction of d-treo-2-methylamino-1-phenyl-1-propanol with 4-morpholylbenzaldehyde in the conditions of convectional heating and microwave activation ru_RU
dc.type Article ru_RU


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